Browsing by Author "Wang, Yiding"
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Item A near-infrared gas sensor system based on tunable laser absorption spectroscopy and its application to CH4/C2H2 detection(SPIE, 2017) He, Qixin; Zheng, Chuantao; Liu, Huifang; Wang, Yiding; Tittel, Frank K.A near-infrared (NIR) dual-channel differential gas sensor system was experimentally demonstrated based on tunable laser absorption spectroscopy (TLAS) and wavelength modulation spectroscopy (WMS). The sensor consists of four modules, including distributed feedback (DFB) lasers for the detection of targeted gases, a custom portable DFB driver compatible for butterfly-packaged DFB lasers, a 20cm-long open-reflective gas-sensing probe and a custom cost-effective lock-in amplifier for harmonic signal extraction. The optical and electrical modules were integrated into a standalone sensor system, which possesses advantages of user-friendly operation, good stability, small volume and low cost. With different DFB lasers, the sensor system can be used to detect different gases. Two DFB diode lasers with emission wavelengths of 1.65 μm and 1.53 μm were used to detect CH4 and C2H2, respectively. Standard CH4 and C2H2 samples were prepared and experiments were carried out to evaluate the performance of the two-gas TLAS sensor system. The relation between the second harmonic amplitudes (2f) and gas concentrations was obtained for the two gases by means of calibration. Both the detection error and the limit of detection (LoD) were determined experimentally. The sensor system will be useful in industrial trace gas monitoring due to its use of a low-loss optical fiber and an open-reflective gas-sensing probe.Item Development and Measurements of a Mid-Infrared Multi-Gas Sensor System for CO, CO2 and CH4 Detection(MDPI, 2017) Dong, Ming; Zheng, Chuantao; Miao, Shuzhuo; Zhang, Yu; Du, Qiaoling; Wang, Yiding; Tittel, Frank K.A multi-gas sensor system was developed that uses a single broadband light source and multiple carbon monoxide (CO), carbon dioxide (CO2) and methane (CH4) pyroelectric detectors by use of the time division multiplexing (TDM) technique. A stepper motor-based rotating system and a single-reflection spherical optical mirror were designed and adopted to realize and enhance multi-gas detection. Detailed measurements under static detection mode (without rotation) and dynamic mode (with rotation) were performed to study the performance of the sensor system for the three gas species. Effects of the motor rotating period on sensor performances were also investigated and a rotation speed of 0.4π rad/s was required to obtain a stable sensing performance, corresponding to a detection period of ~10 s to realize one round of detection. Based on an Allan deviation analysis, the 1σ detection limits under static operation are 2.96, 4.54 and 2.84 parts per million in volume (ppmv) for CO, CO2 and CH4, respectively and the 1σ detection limits under dynamic operations are 8.83, 8.69 and 10.29 ppmv for the three gas species, respectively. The reported sensor has potential applications in various fields requiring CO, CO2 and CH4 detection such as in coal mines.Item Double-range near-infrared acetylene detection using a dual spot-ring Herriott cell (DSR-HC)(Optical Society of America, 2018) Dong, Ming; Zheng, Chuantao; Yao, Dan; Zhong, Guoqiang; Miao, Shuzhuo; Ye, Weilin; Wang, Yiding; Tittel, Frank K.Design and fabrication of a dual spot-ring Herriott cell (DSR-HC) were proposed. The sealed Herriott cell with a dimensional size of 5.5 cm × 9.2 cm × 32.1 cm, possessed two input/output coupling holes leading to two absorption path lengths of ~20 m and ~6 m, respectively. An acetylene (C2H2) sensor system with a double-range was developed using the DSR-HC and wavelength modulation spectroscopy (WMS) technique. A near-infrared distributed feedback (DFB) laser was employed for targeting a C2H2 absorption line at 6521.2 cm-1. C2H2concentration measurements were carried out by modulating the laser at a 5 kHz frequency and demodulating the detector signal with LabVIEW software. An Allan-Werle deviation analysis indicated that the limit of detection (LoD) for the two absorption path lengths of 20 m and 6 m are 7.9 parts-per-million in volume (ppmv) and 4.0 ppmv, respectively. The DSR-HC concept can be used to fabricate similar cells for single-gas detection requiring two different detection ranges as well as for dual-gas detection requiring different absorption path lengths.Item Dual-feedback mid-infrared cavity-enhanced absorption spectroscopy for H2CO detection using a radio-frequency electrically-modulated interband cascade laser(The Optical Society, 2018) He, Qixin; Zheng, Chuantao; Lou, Minhan; Ye, Weilin; Wang, Yiding; Tittel, Frank K.A mid-infrared cavity-enhanced sensor system was demonstrated for the detection of formaldehyde (H2CO) using a continuous-wave (cw) interband cascade laser (ICL) centered at 3599 nm. A compact Fabry-Perot (F-P) cavity with a physical size of 38 × 52 × 76 mm3 was developed consisting of two concave mirrors with a radius of curvature of 80 mm and a reflectivity of 99.8% at 3.6 μm. Different from the widely reported electro-optical (EO) external modulation based Pound-Drever-Hall (PDH) locking technique, a radio-frequency electrical internal modulation based PDH technique was used for locking the laser mode to the cavity mode. A dual-feedback control on the laser current and on the piezo transducer (PZT) displacement was utilized for further stabilizing mode locking. A 20 m effective optical path length was achieved with a cavity length of 2 cm and a finesse of 1572. The effectiveness and sensitivity of the sensor system were demonstrated by targeting an absorption line at 2778.5 cm−1 for H2CO measurements. A linear relation between the cavity transmitted signal amplitude and the H2CO concentration was obtained within the range of 0−5 ppm. A 1σ detection limit of 25 parts-per-billion (ppb) was achieved with an averaging time of 1 s based on Allan-Werle variance analysis. The reported dual-feedback RF modulation based PDH technique led to a method for gas detection using a similar experimental setup and measurement scheme.Item ICL-based mid-infrared carbon dioxide sensor system for deep-sea natural gas hydrate exploration(Optical Society of America, 2019) Liu, Zhiwei; Zheng, Chuantao; Chen, Chen; Li, Yafei; Xie, Hongtao; Ren, Qiang; Wang, Yiding; Tittel, Frank K.For deep-sea natural gas hydrate exploration, highly sensitive detection of the dissolved gas in seawater near the seabed is significant because it requires the sensor system to be small in size, low in power consumption, and high in sensitivity. A mid-infrared sensor system was developed to detect dissolved carbon dioxide (CO2) in sea-water, while employing a 4319 nm continuous-wave interband cascade laser (ICL) and a multi-pass gas cell (MPGC) with a 29.8 m optical path length. A compact rectilinear optical structure was proposed by using the free-space-emitting ICL and tunable laser absorption spectroscopy (TLAS). This leads to a minimized sensor size and a simple optical alignment for deep-sea operation. A strong CO2 absorption line, located at 2315.19 cm−1 and a weak 2315.28 cm−1 line and at a low pressure of 40 Torr, was targeted for low- and high-concentration CO2 detection within a concentration range of 0-1000 parts per billion by volume (ppbv) and 0-40 parts per million by volume (ppmv), respectively. The limit of detection (LoD) was assessed to be 0.72 ppbv at an averaging time of 2 s, and the response time was measured to be ~30 s at a flow rate of ~180 standard cubic centimeters per minute (sccm). Deployment of the CO2 sensor combined with a gas-liquid separator was carried out for the CO2 detection in the gas extracted from water, which validated the reported sensor system’s potential application for deep-sea natural gas hydrate exploration.Item Interband cascade laser based mid-infrared methane sensor system using a novel electrical-domain self-adaptive direct laser absorption spectroscopy (SA-DLAS)(Optical Society of America, 2017) Song, Fang; Zheng, Chuantao; Yan, Wanhong; Ye, Weilin; Wang, Yiding; Tittel, Frank K.To suppress sensor noise with unknown statistical properties, a novel self-adaptive direct laser absorption spectroscopy (SA-DLAS) technique was proposed by incorporating a recursive, least square (RLS) self-adaptive denoising (SAD) algorithm and a 3291 nm interband cascade laser (ICL) for methane (CH4) detection. Background noise was suppressed by introducing an electrical-domain noise-channel and an expectation-known-based RLS SAD algorithm. Numerical simulations and measurements were carried out to validate the function of the SA-DLAS technique by imposing low-frequency, high-frequency, White-Gaussian and hybrid noise on the ICL scan signal. Sensor calibration, stability test and dynamic response measurement were performed for the SA-DLAS sensor using standard or diluted CH4ﾠsamples. With the intrinsic sensor noise considered only, an Allan deviation of ~43.9 ppbv with a ~6 s averaging time was obtained and it was further decreased to 6.3 ppbv with a ~240 s averaging time, through the use of self-adaptive filtering (SAF). The reported SA-DLAS technique shows enhanced sensitivity compared to a DLAS sensor using a traditional sensing architecture and filtering method. Indoor and outdoor atmospheric CH4measurements were conducted to validate the normal operation of the reported SA-DLAS technique.Item Light-induced off-axis cavity-enhanced thermoelastic spectroscopy in the near-infrared for trace gas sensing(Optical Society of Americ, 2021) Zheng, Kaiyuan; Zheng, Chuantao; Zheng, Chuantao; Hu, Lien; Guan, Gangyun; Ma, Yanming; Song, Fang; Zhang, Yu; Zhang, Yu; Wang, Yiding; Tittel, Frank K.A trace gas sensing technique of light-induced off-axis cavity-enhanced thermoelastic spectroscopy (OA-CETES) in the near-infrared was demonstrated by combing a high-finesse off-axis integrated cavity and a high Q-factor resonant quartz tuning fork (QTF). Sensor parameters of the cavity and QTF were optimized numerically and experimentally. As a proof-of-principle, we employed the OA-CETES for water vapor (H2O) detection using a QTF (Q-factor ∼12000 in atmospheric pressure) and a 10cm-long Fabry-Perot cavity (finesse ∼ 482). By probing a H2O line at 7306.75 cm-1, the developed OA-CETES sensor achieved a minimum detection limit (MDL) of 8.7 parts per million (ppm) for a 300 ms integration time and a normalized noise equivalent absorption (NNEA) coefficient of 4.12 × 10−9cm-1 WHz-1/2. Continuous monitoring of indoor and outdoor atmospheric H2O concentration levels was performed for verifying the sensing applicability. The realization of the proposed OA-CETES technique with compact QTF and long effective path cavity allows a class of optical sensors with low cost, high sensitivity and potential for long-distance and multi-point sensing.Item Long-distance in-situ methane detection using near-infrared light-induced thermo-elastic spectroscopy(Elsevier, 2021) Hu, Lien; Zheng, Chuantao; Zhang, Minghui; Zheng, Kaiyuan; Zheng, Jie; Song, Zhanwei; Li, Xiuying; Zhang, Yu; Wang, Yiding; Tittel, Frank K.A wavelength-locked light-induced thermo-elastic spectroscopy (WL-LITES) gas sensor system was proposed for long-distance in-situ methane (CH4) detection using a fiber-coupled sensing probe. The wavelength-locked scheme was used to speed the sensor response without scanning the laser wavelength across the CH4 absorption line. A small-size piezoelectric quartz tuning fork (QTF) with a wide spectral response range was adopted to enhance the photo-thermal signal. The optical excitation parameters of the QTF were optimized based on experiment and simulation for improving the signal-to-noise ratio of the LITES technique. An Allan deviation analysis was employed to evaluate the limit of detection of the proposed sensor system. With a 0.3 s lock-in integration time and a ∼ 100 m optical fiber, the WL-LITES gas sensor system demonstrates a minimum detection limit (MDL) of ∼ 11 ppm in volume (ppmv) for CH4 detection, and the MDL can be further reduced to ∼ 1 ppmv with an averaging time of ∼ 35 s. A real-time in-situ monitoring of CH4 leakage reveals that the proposed sensor system can realize a fast response (< 12 s) for field application.Item Mid-infrared chalcogenide slot waveguide plasmonic resonator sensor embedded with Au nanorods for surface-enhanced infrared absorption spectroscopy(Elsevier, 2022) Pi, Mingquan; Zhao, Huan; Li, Chunguang; Min, Yuting; Peng, Zihang; Ji, Jialin; Huang, Yijun; Song, Fang; Liang, Lei; Zhang, Yu; Wang, Yiding; Tittel, Frank K.; Zheng, ChuantaoThe problem of a traditional waveguide plasmonic resonator sensor is that part of the near-field intensity enhanced area is confined in the waveguide dielectric layer, which decreases the interaction effect between light and analyte. In order to solve this problem, a novel mid-infrared (MIR) chalcogenide (ChG) slot waveguide plasmonic resonator (SWGPR) sensor embedded with Au nanorods was proposed, where Au nanorods were used as antenna for enhancing mode coupling with the waveguide through resonance at the absorption wavelength of the analyte. The antenna parameters were optimized to make the resonance wavelength align with the absorption wavelength of the analyte. The proposed waveguide structure provides a sufficient sensing area and increases the electric field enhancement factor to > 6400. Polymethyl methacrylate (PMMA) and styrene were adopted as the analyte for sensing performance evaluation. The normalized absorption reaches 23.31 when the maximum extinction coefficient of PMMA is 0.08, which is at least 7 times higher than other silicon-on-insulator (SOI) waveguide plasmonic resonator sensors. The proposed waveguide structure provides a new idea for the design of other waveguide plasmonic resonator sensors with high sensing performance and has the potential for biochemical sensing.Item Near-infrared acetylene sensor system using off-axis integrated-cavity output spectroscopy and two measurement schemes(Optical Society of America, 2018) Zheng, Kaiyuan; Zheng, Chuantao; He, Qixin; Yao, Dan; Hu, Lien; Zhang, Yu; Wang, Yiding; Tittel, Frank K.For highly sensitive and accurate acetylene (C2H2) detection, a near-infrared (NIR) off-axis integrated-cavity output spectroscopy (OA-ICOS) sensor system based on an ultra-compact cage-based absorption cell was proposed. The absorption cell with dimensions of 10 cm × 8 cm × 6 cm realized a dense-pattern and an easily-aligned stable optical system. The OA-ICOS sensor system employed a 6cm-long optical cavity that was formed by two mirrors with a reflectivity of 99.35% and provided an effective absorption path length of ∼9.28 m. The performance of the C2H2 sensor system based on two measurement schemes, i.e. laser direct absorption spectroscopy (LDAS) and wavelength modulation spectroscopy (WMS) is reported. A NIR distributed feedback (DFB) laser was employed for targeting a C2H2 absorption line at 6523.88 cm−1. An Allan deviation analysis yielded a detection sensitivity of 760 parts-per-billion in volume (ppbv) for an averaging time of 304 s using the LDAS-based OA-ICOS. A detection sensitivity of 85 ppbv for an averaging time of 250 s was obtained using the WMS-based OA-ICOS, which was further improved by a factor of ~9 compared to the result obtained with the LDAS method. The proposed sensor system has the advantages of reduced size and cost with acceptable detection sensitivity, which is suitable for applications in trace gas sensing in harsh environments and weight-limited balloon-embedded observations.Item Near-Infrared Dual-Gas Sensor System for Methane and Ethane Detection Using a Compact Multipass Cell(Frontiers Media S.A., 2022) Xi, Zhenhai; Zheng, Kaiyuan; Zheng, Chuantao; Zhang, Haipeng; Song, Fang; Li, Chunguang; Ye, Weilin; Zhang, Yu; Wang, Yiding; Tittel, Frank K.In this invited paper, a compact dense-pattern multipass cell-based near-infrared sensor system was demonstrated for detection of parts-per-billion in volume (ppbv)-level methane (CH4) and ethane (C2H6). The dimension size of the fabricated gas cell is 18.5 × 8 × 9 cm3 with an absorption path length of 9.39 m. CH4 measurement was realized within a spectral range of 6,046–6,048 cm−1 and an absorption line of 6,046.95 cm−1. The spectral range for C2H6 detection is 5,951–5,953 cm−1 with an absorption line of 5,951.73 cm−1. Allan deviation analysis was used for evaluating the dual-gas sensing performance, and a detection limit of 78 ppbv for CH4 and 190 ppbv for C2H6 were achieved, respectively, with an averaging time of 0.8 s. Furthermore, CH4 measurement in the indoor and outdoor atmosphere was both performed to verify the field sensing capability of the sensor system. Compared with two separate sensor systems for CH4/C2H6 sensing, the proposed dual-gas sensor system using two near-infrared lasers and one multipass cell has the advantages of low-cost, compact-size without decreasing the selectivity and sensitivity.Item On-chip mid-infrared silicon-on-insulator waveguide methane sensor using two measurement schemes at 3.291 μm(Frontiers Media S.A., 2022) Zhao, Huan; Zheng, Chuantao; Pi, Mingquan; Liang, Lei; Song, Fang; Zhang, Yu; Wang, Yiding; Tittel, Frank K.Portable or even on-chip detection of methane (CH4) is significant for environmental protection and production safety. However, optical sensing systems are usually based on discrete optical elements, which makes them unsuitable for the occasions with high portability requirement. In this work, we report on-chip silicon-on-insulator (SOI) waveguide CH4 sensors at 3.291 μm based on two measurement schemes including direct absorption spectroscopy (DAS) and wavelength modulation spectroscopy (WMS). In order to suppress noise, Kalman filter was adopted in signal processing. By optimizing the waveguide cross-section structure, an etch depth of 220 nm was selected with an experimentally high power confinement factor (PCF) of 23% and a low loss of only 0.71 dB/cm. A limit of detection (LoD) of 155 parts-per-million (ppm) by DAS and 78 ppm by WMS at an averaging time of 0.2 s were obtained for a 2 cm-long waveguide sensor. Compared to the chalcogenide (ChG) waveguide CH4 sensors at the same wavelength, the reported sensor reveals the minimum waveguide loss and the lowest LoD. Therefore the SOI waveguide sensor has the potential of on-chip gas sensing in the mid-infrared (MIR) waveband.Item Performance Enhancement of Methane Detection Using a Novel Self-Adaptive Mid-Infrared Absorption Spectroscopy Technique(IEEE, 2018) Song, Fang; Zheng, Chuantao; Yan, Wanhong; Ye, Wei Lin; Zhang, Yu; Wang, Yiding; Tittel, Frank K.An electrical-domain self-adaptive mid-infrared absorption spectroscopy for methane detection based on an interband cascade laser was demonstrated. By adding noise into the laser drive signal, denoising and sensing performances were evaluated for the technique. Experiments were made to study the effects of noise level/type on sensor stability, characterized by Allan deviation. High- and low-frequency noise levels have the same functional variation trend on Allan deviation, which differs from white Gaussian noise. Within a noise level range of 0-125 mV for low- and high-frequency noise and 0-62.5 mV for white Gaussian noise in the mercury-cadmium-telluride detector's output (with a pure signal amplitude of ~300 mV), the sensor stability using self-adaptive denoising was enhanced by a factor of 1.05-20, 1.32-6.25, and 1.15-3.33 times compared to that using no filtering, for the three kinds of noise, respectively. The reported self-adaptive methane sensor system shows enhanced stability compared to the direct laser absorption spectroscopy sensor using traditional sensing architecture and classic filtering method. The sensor was further evaluated through outdoor atmospheric methane measurements using such technique. A second-order self-adaptive direct laser absorption spectroscopy technique was also proposed for noise suppression in both optical and electrical domain as an outlook of the concept of this paper.Item Ppbv-Level Ethane Detection Using Quartz-Enhanced Photoacoustic Spectroscopy with a Continuous-Wave, Room Temperature Interband Cascade Laser(MDPI, 2018) Li, Chunguang; Dong, Lei; Zheng, Chuantao; Lin, Jun; Wang, Yiding; Tittel, Frank K.A ppbv-level quartz-enhanced photoacoustic spectroscopy (QEPAS)-based ethane (C2H6) sensor was demonstrated by using a 3.3 μm continuous-wave (CW), distributed feedback (DFB) interband cascade laser (ICL). The ICL was employed for targeting a strong C2H6 absorption line located at 2996.88 cm−1 in its fundamental absorption band. Wavelength modulation spectroscopy (WMS) combined with the second harmonic (2f) detection technique was utilized to increase the signal-to-noise ratio (SNR) and simplify data acquisition and processing. Gas pressure and laser frequency modulation depth were optimized to be 100 Torr and 0.106 cm−1, respectively, for maximizing the 2f signal amplitude. Performance of the QEPAS sensor was evaluated using specially prepared C2H6 samples. A detection limit of 11 parts per billion in volume (ppbv) was obtained with a 1-s integration time based on an Allan-Werle variance analysis, and the detection precision can be further improved to ~1.5 ppbv by increasing the integration time up to 230 s.Item Repetitively Mode-Locked Cavity-Enhanced Absorption Spectroscopy (RML-CEAS) for Near-Infrared Gas Sensing(MDPI, 2017) He, Qixin; Lou, Minhan; Zheng, Chuantao; Ye, Weilin; Wang, Yiding; Tittel, Frank K.A Pound-Drever-Hall (PDH)-based mode-locked cavity-enhanced sensor system was developed using a distributed feedback diode laser centered at 1.53 µm as the laser source. Laser temperature scanning, bias control of the piezoelectric ceramic transducer (PZT) and proportional-integral-derivative (PID) feedback control of diode laser current were used to repetitively lock the laser modes to the cavity modes. A gas absorption spectrum was obtained by using a series of absorption data from the discrete mode-locked points. The 15 cm-long Fabry-Perot cavity was sealed using an enclosure with an inlet and outlet for gas pumping and a PZT for cavity length tuning. The performance of the sensor system was evaluated by conducting water vapor measurements. A linear relationship was observed between the measured absorption signal amplitude and the H2O concentration. A minimum detectable absorption coefficient of 1.5 × 10–8 cm–1 was achieved with an averaging time of 700 s. This technique can also be used for the detection of other trace gas species by targeting the corresponding gas absorption line.Item Review of Incoherent Broadband Cavity-Enhanced Absorption Spectroscopy (IBBCEAS) for Gas Sensing(MDPI, 2018) Zheng, Kaiyuan; Zheng, Chuantao; Zhang, Yu; Wang, Yiding; Tittel, Frank K.Incoherent broadband cavity-enhanced absorption spectroscopy (IBBCEAS) is of importance for gas detection in environmental monitoring. This review summarizes the unique properties, development and recent progress of the IBBCEAS technique. Principle of IBBCEAS for gas sensing is described, and the development of IBBCEAS from the perspective of system structure is elaborated, including light source, cavity and detection scheme. Performances of the reported IBBCEAS sensor system in laboratory and field measurements are reported. Potential applications of this technique are discussed.Item Slow-light-enhanced on-chip 1D and 2D photonic crystal waveguide gas sensing in near-IR with an ultrahigh interaction factor(Optica Publishing Group, 2023) Peng, Zihang; Huang, Yijun; Zheng, Kaiyuan; Zheng, Chuantao; Pi, Mingquan; Zhao, Huan; Ji, Jialin; Min, Yuting; Liang, Lei; Song, Fang; Zhang, Yu; Wang, Yiding; Tittel, Frank K.Nanophotonic waveguides hold great promise to achieve chip-scale gas sensors. However, their performance is limited by a short light path and small light–analyte overlap. To address this challenge, silicon-based, slow-light-enhanced gas-sensing techniques offer a promising approach. In this study, we experimentally investigated the slow light characteristics and gas-sensing performance of 1D and 2D photonic crystal waveguides (PCWs) in the near-IR (NIR) region. The proposed 2D PCW exhibited a high group index of up to 114, albeit with a high propagation loss. The limit of detection (LoD) for acetylene (C2H2) was 277 parts per million (ppm) for a 1 mm waveguide length and an averaging time of 0.4 s. The 1D PCW shows greater application potential compared to the 2D PCW waveguide, with an interaction factor reaching up to 288%, a comparably low propagation loss of 10 dB/cm, and an LoD of 706 ppm at 0.4 s. The measured group indices of the 2D and 1D waveguides are 104 and 16, respectively, which agree well with the simulation results.